CN101401818A - Sada mechanized forging process - Google Patents

The invention belongs to the Tibetan-medicine field, which particularly relates to a Zote (btso-thal) mechanical processing technique. In the invention, the prior Zote (btso-thal) processing method is divided into three unit operations of mixing, liquid-liquid separation and distillation reflux, the electrically mechanical stirring replaces the prior manual solid-liquid, liquid-liquid and solid-solid grinding, the liquid pumping by a motor driven pump replaces the prior upper-layer liquid decantation(dumping) type liquid-liquid separation, and the reflux with environmental protection and energy conservation replaces the prior open type decoction. All working procedures are performed at a negative pressure state, thereby effectively avoiding the damage to an operator due to the spillover of mercury steam; and in the invention, all gases and auxiliary materials contacting mercury are allowed to enter a municipal treatment system after purified. The inventor finds that by adopting the technique to process the Zote (btso-thal), the urinary mercury of the operator is not obviously changed before and after processing. The technique has the advantages of environmental protection, no damage to the operator, short production cycle (2 to 3 weeks), stable product quality, low production cost, high production efficiency, low labor intensity, obvious economic and social benefits and the like.

A kind of ZUOTAI mechanization processing procedure

One, technical field:

The invention belongs to the Tibetan medicine field, relate in particular to the mechanization processing procedure of ZUOTAI.

Two, technical background: ZUOTAI is to be the Tibetan medicine material commonly used that can directly be used as medicine that raw material is made through certain processing procedure with hydrargyrum, is the Tibetan language transliteration.ZUOTAI is the primary raw material of many famous and precious Tibetan medicines, and long history is arranged in the use of Tibetan medicine, and application quantity is big, use is wide.The tradition Tibetan medicine thinks through the hydrargyrum of concocting, single with or prepare other medicines and can control various diseases, have the effect of granulation promoting spleen invigorating, strengthening by means of tonics and disease-resistant body-building.According to the data record, the process of preparing Chinese medicine of hydrargyrum mainly contains white method for making, violent method for making, hot method for making, cold method for making etc.Wherein, just professor youth translates the cold method for making of putting in order out through facts have proved, and is effective.The inventor investigates discovery, and existing ZUOTAI is concocted and is in original workshop form basically, based on manually-operated; The production equipment of critical process falls behind, and mechanization degree is low; Production process is mainly controlled by the experience of Producer, difficult quality control.Just because of this, operator's health in concocting process is subjected to very big harm, as after concocting ZUOTAI, and many operators' urine hydrargyrum exceeds surplus the normal value 50 times, symptoms such as headache, dizzy and tinnitus occur; Labor intensity is very big, as concocts 50 kilograms of hydrargyrums, and whole people surplus the requirementss of process 30 day just can finish surplus the manual labour 50 round the clock.In addition, traditional processing procedure environmental pollution is serious etc.

Three, summary of the invention

The objective of the invention is at the prior art above shortcomings, in conjunction with modern pharmaceutical science and technology and successful experience, the ZUOTAI mechanization processing procedure of developing.This technology and method can effectively overcome the prior art above shortcomings, it has environmental friendliness,, advantage such as production cycle foreshorten to 2-3 week, constant product quality, production cost low, production efficiency high and labor intensity little little to the human injury, and remarkable economical and social benefit are arranged.

Technical scheme: the technological process of ZUOTAI mechanization processing procedure is that hydrargyrum mixes with the liquid-solid of three hot powder, the liquid-liquid separation of hydrargyrum and three Xin Fenshui; Hydrargyrum mixes with the liquid-solid of Sal, trona, the liquid-liquid separation of hydrargyrum and Sal, trona water; Hydrargyrum mixes with the liquid-liquid of urine of baby boys, the liquid-liquid separation of hydrargyrum and urine of baby boys; Hydrargyrum mixes with the liquid-liquid of trona, Fructus Hippophae water, the liquid-liquid separation of hydrargyrum and trona, Fructus Hippophae water; Hydrargyrum mixes with the liquid-liquid of stallion urine, Fructus Hippophae water, the liquid-liquid separation of hydrargyrum and stallion urine, Fructus Hippophae water; Hydrargyrum mixes with the liquid-liquid of cattle urine, Fructus Hippophae water, the liquid-liquid separation of hydrargyrum and cattle urine, Fructus Hippophae water; Hydrargyrum mixes with the liquid-liquid of Alumen preparata, fibroferritum water, the liquid-liquid separation of hydrargyrum and Alumen preparata, fibroferritum water; Hydrargyrum mixes with the liquid-liquid of Borax, healthy middle-aged male urine, the liquid-liquid separation of hydrargyrum and Borax, healthy middle-aged male urine; Hydrargyrum mixes with the liquid-liquid of natural salt, tibet red salt, nitre, thenardite, Natrii Sulfas, Sal, trona, Fructus Hippophae water, the liquid-liquid separation of hydrargyrum and natural salt, tibet red salt, nitre, thenardite, Natrii Sulfas, Sal, trona, Fructus Hippophae water; Hydrargyrum mixes with liquid-liquid of cellar, Fructus Hippophae water, Alumen preparata Tu Shui, the liquid-liquid separation of hydrargyrum and cellar, Fructus Hippophae water, Alumen preparata Tu Shui; Hydrargyrum mixes with the liquid-liquid of a watt powder cream, Fructus Hippophae water, the liquid-liquid separation of hydrargyrum and watt powder cream, Fructus Hippophae water; Hydrargyrum mixes with the liquid-liquid of fresh cellar, the liquid-liquid separation of hydrargyrum and fresh cellar; Hydrargyrum mixes with the liquid-liquid of Bulbus Allii water, the liquid-liquid separation of hydrargyrum and Bulbus Allii water; Hydrargyrum mixes with the liquid-liquid of beef water, the liquid-liquid separation of hydrargyrum and beef water; Hydrargyrum mixes with the liquid-liquid of butter water, the liquid-liquid separation of hydrargyrum and butter water; Hydrargyrum with coagulate mixed liquor, black earth vitriol water, Fructus Hippophae water, the cellar distillation and reflux in broken Mirabilitum crystallina that leather gets by Adeps Naemorhedi, woodchuck oil, Medulla Bovis seu Bubali, sheep bone marrow, milk, hydrargyrum and the liquid-liquid separation that coagulates mixed liquor that leather gets, black earth vitriol water, Fructus Hippophae water, cellar by Adeps Naemorhedi, woodchuck oil, Medulla Bovis seu Bubali, sheep bone marrow, milk; Hydrargyrum and the solution that makes by Bayuan powder and another name of the sun head powder, black earth vitriol water, Fructus Hippophae water, cellar, blue or green oil distillation and reflux in Mirabilitum crystallina, the liquid-liquid separation of hydrargyrum and the solution that makes by Bayuan powder and another name of the sun head powder, black earth vitriol water, Fructus Hippophae water, cellar, blue or green oil; Hydrargyrum and eight bronzes, Radix Aconiti Kusnezoffii powder, Oleum Tiglii, black blue or green oil distillation and reflux in broken Mirabilitum crystallina, the liquid-liquid separation of hydrargyrum and eight bronzes, Radix Aconiti Kusnezoffii powder, Oleum Tiglii, black blue or green oil; The liquid-solid of hydrargyrum and Cosan is mixed to blue black, admittedly blue black powder and eight bronzes, Bayuan powder, an amount of warm water consolidate-mix the ZUOTAI product.Can increase the operation of washing water purification silver behind the liquid-liquid separation.Washing water purification silver is the process that impurity is removed in the hydrargyrum washing after to liquid-liquid separation of water or warm water.Hydrargyrum spends the night when depositing, and steep with the Fructus Hippophae water logging.The present invention is in order to prevent that mercury vapor overflows the harm operator in the concocting process, and all process steps is all operated in the hermetic container of negative pressure state.

Process conditions be hydrargyrum with liquid-solid mixing of three hot powder in electronic mixing time be 4～24 hours, rotating speed is 30～480rpm, color stops after becoming bottle green or blackish green, three hot powder are abbreviations of Rhizoma Alpiniae Officinarum, bamboo or wicker fence book box, three kinds of medical materials of Fructus Piperis; Electronic mixing time in liquid-solid mixing of hydrargyrum and Sal, trona is 1～9 hour, and rotating speed is 30～480rpm, and color becomes Dark grey and stops; Hydrargyrum is 1～9 hour with electronic mixing time during the liquid-liquid of urine of baby boys mixes, and rotating speed is 60～540rpm, and urine of baby boys should use in back 15 days in collection; Hydrargyrum is 1～9 hour with electronic mixing time during the liquid-liquid of trona, Fructus Hippophae water mixes, and rotating speed is 60～540rpm; Electronic mixing time during the liquid-liquid of hydrargyrum and stallion urine, Fructus Hippophae water mixes is 1～24 hour, and rotating speed is 60～540rpm, mixes three times.Stallion urine should use in back 15 days in collection.Electronic mixing time during the liquid-liquid of hydrargyrum and cattle urine, Fructus Hippophae water mixes is 1～4 hour, and rotating speed is 60～540rpm, mixes three times, and cattle urinates should be in use in back 15 days of the collection; Hydrargyrum is 1～4 hour with electronic mixing time during the liquid-liquid of Alumen preparata, fibroferritum water mixes, and rotating speed is 60～540rpm, mixes three times; Electronic mixing time during the liquid-liquid of hydrargyrum and Borax, healthy middle-aged male urine mixes is 1～4 hour, and rotating speed is 60～540rpm; Hydrargyrum is 1～4 hour with electronic mixing time during the liquid-liquid of natural salt, tibet red salt, nitre, thenardite, Natrii Sulfas, Sal, trona, Fructus Hippophae water mixes, and rotating speed is 60～540rpm, mixes three times; Hydrargyrum is 1～4 hour with electronic mixing time during liquid-liquid of cellar, Fructus Hippophae water, Alumen preparata Tu Shui mixes, and rotating speed is 60～540rpm, mixes three times; Hydrargyrum and electronic mixing time during the liquid-liquid of a watt powder cream, Fructus Hippophae water mixes 1～4 hour, rotating speed is 60～540rpm, mixes three times.Hydrargyrum is 1～4 hour with electronic mixing time during the liquid-liquid of fresh cellar mixes, and rotating speed is 60～540rpm, and mixing temperature is 15～35 ℃, mixes twice; Hydrargyrum is 1～4 hour with electronic mixing time during the liquid-liquid of Bulbus Allii water mixes, and rotating speed is 60～540rpm, mixes four times; Hydrargyrum is 1～2 hour with electronic mixing time during the liquid-liquid of beef water mixes, and rotating speed is 60～540rpm, mixes twice; Hydrargyrum is 1～2 hour with mixing time during the liquid-liquid of butter water mixes, and rotating speed is 60～540rpm, mixes twice; Hydrargyrum is 12～72 hours with coagulating mixed liquor, black earth vitriol water, Fructus Hippophae water, the cellar response time in the distillation and reflux in broken Mirabilitum crystallina that leather gets by Adeps Naemorhedi, woodchuck oil, Medulla Bovis seu Bubali, sheep oil, milk, and temperature is 80～150 ℃; Hydrargyrum is 12～48 hours with the solution that is made by Bayuan powder and another name of the sun head powder, black earth vitriol water, Fructus Hippophae water, cellar, blue or green oil response time in the distillation and reflux in Mirabilitum crystallina, temperature is 80～150 ℃, and Bayuan powder is the abbreviation of Pyritum, Gold Ore, silver ore, Magnetitum, Alumen, sulphur, Realgar, Muscovitum Bayuan powder Ore; Hydrargyrum and eight bronzes, Radix Aconiti Kusnezoffii powder, Oleum Tiglii, black blue or green oil response time in the distillation and reflux in Mirabilitum crystallina are 6～24 hours, temperature is 120～220 ℃, and eight bronzes are general names of the powder of eight kinds of mineral such as gold, silver, copper, ferrum, one-tin brass, rose copper, black and white aluminium powder; Hydrargyrum is 6～48 hours with mixing time during Cosan mixes, and temperature is a room temperature, lucifuge; Gu blue black powder and eight bronzes, Bayuan powder, the electronic mixing time in consolidate-the mixing of warm water is 12～48 hours in right amount; All process steps of the present invention is all operated in-0.1～-0.5 atmospheric hermetic container, and negative pressure state realizes from the hermetic container continuous air extraction by Vacuum Pumps Station.All materials that the aerofluxus of Vacuum Pumps Station reaches and hydrargyrum is contacted must be through the purified treatment and the municipal processing system of being allowed for access after the assay was approved.

The present invention is to improve on the 88107006.8 disclosed hydrargyrum processing methods in the patent No..Mixing of the present invention is meant the process of the electronic stirring of material in hermetic container.State according to material, Gu mixing and being divided into liquid-solid mixing is that liquid-solid mixes, liquid-liquid mixing is that liquid-liquid mixing and solid-mixing are that solid-solid mixes, mix with being mixed into of three hot powder is liquid-solid as hydrargyrum, hydrargyrum mixes with the liquid-liquid that is mixed into of urine of baby boys, consolidate-mixes with being mixed into of eight bronzes, Bayuan powder Gu hydrargyrum mixes back gained blue powder with Cosan again.Solid liquid-solid mixing, solid-mixing can be finished in mixers such as trough-type mixture machine, cone-type spiral mixer, ball mill, and liquid-liquid mixing can be finished in material is the equipment such as stirred tank, reactor, reactor of rustless steel, enamel and glass etc.Separation of the present invention be meant that hydrargyrum mixes with adjuvant or distillation and reflux after the process that is separated from each other.Because the density contrast of hydrargyrum and adjuvant is very big, in case stop to stir, liquid adjuvant can be very fast and the hydrargyrum natural layering, adjuvant also can be very fast and the hydrargyrum natural layering under the suspension effect of water for solid-state adjuvant, then, utilize negative pressure that supernatant liquid is extracted out, adjuvant was finished fast and efficiently with just separating of hydrargyrum.Washing water purification silver can be decomposed into that hydrargyrum mixes with the liquid-liquid of water, two steps of liquid-liquid separation of hydrargyrum and water.Distillation and reflux of the present invention is exactly the process that flows back to reactor at the steam that the reactor internal reaction that condensing unit is installed produces through condensation.Distillation and reflux can prevent that the evaporation of effective ingredient and hydrargyrum from overflowing, and can finish in the Chinese medicine extraction device.

In sum, the present invention is resolved into mixing, liquid-liquid separation, three kinds of unit operationss of distillation and reflux with traditional ZUOTAI concocting method, admittedly stir alternative original manual solid-liquid, liquid-liquid, consolidate-mill with motor machine, with the liquid-liquid separation of alternative original supernatant liquid decant (falling) formula of electrodynamic pump drawing liquid, substitute original open decoction with environmental protection, energy-conservation distillation and reflux.That new technology has is with short production cycle, the advantage of operator's light labor intensity, energy-conservation and constant product quality.What be worth emphasizing is that all process steps of the present invention is all operated under negative pressure state, can avoid mercury vapor to overflow the harm operator effectively.The inventor finds, adopts this technology to concoct ZUOTAI, does not have significant change before and after operator's urine hydrargyrum is concocted.Again since with the contacted gas of hydrargyrum, adjuvant etc. must be through the purified treatment municipal processing system of being allowed for access, therefore, this process environments close friend.

Four, the specific embodiment

Embodiment one

Hydrargyrum mixes with the liquid-solid of three hot powder: it is that 150 liters, material are in the vertical spiral ribbon mixer of 361L that volume is gone in 5.50 kilograms of Fructus Piperis Longi powder, 4.00 kilograms of Rhizoma Alpiniae Officinarum powder, 5.00 kilograms of Fructus Piperis powders and 50.00 kg of water snow covers, open electronic stirring, when color becomes bottle green, stopped in 4 hours in stirring under the 480rpm rotating speed.

The liquid-liquid separation of hydrargyrum and three Xin Fenshui: in vertical spiral ribbon mixer, inject 30 liters of 70 ℃ of hot water, open electronic stirring, after stirring under the 30rpm rotating speed stops after 10 minutes, treats supernatant liquid and hydrargyrum layering, supernatant liquid is extracted out with the granule pump.The liquid of extracting out is treated the unified purified treatment in back.

Hydrargyrum mixes with the liquid-solid of Sal, trona: reinstall 25.00 kilograms of Sal, 25.00 kilograms of trona in vertical spiral ribbon mixer, open electronic stirring, stop after stirring 1 hour under the 480rpm rotating speed.

Hydrargyrum and Sal, trona water liquid-liquid separation: in the vertical helical mixer, inject 20.00 liters of 70 ℃ of hot water, open electronic stirring, after stirring 15 minutes under the 30rpm rotating speed, stop, after treating supernatant liquid and hydrargyrum layering, with the granule pump supernatant liquid is extracted out, open bottom valve then, hydrargyrum is discharged in the container of subsequent processing.The liquid of extracting out is treated the unified purified treatment in back.

Hydrargyrum mixes with the liquid-liquid of urine of baby boys: toward 8.00 liters of urine of baby boys that the interior injection of 50 liters of double-layer glass reaction kettles that fill hydrargyrum was gathered before 15 days, open electronic stirring, stop after stirring 1 hour under the 540rpm rotating speed.

The liquid-liquid separation of hydrargyrum and urine of baby boys: after treating upper strata urine of baby boys and hydrargyrum layering, the negative pressure of utilizing Vacuum Pumps Station to produce is extracted supernatant liquid out.The liquid of extracting out is treated the unified purified treatment in back.

Hydrargyrum mixes with the liquid-liquid of trona, Fructus Hippophae water: pack in the double glazing reactor that fills hydrargyrum 0.10 kilogram of trona and 10.00 liters of Fructus Hippophae water, open electronic stirring, and after stirring 1 hour under the 540rpm rotating speed, stop.

The liquid-liquid separation of hydrargyrum and trona, Fructus Hippophae water: after treating supernatant liquid and hydrargyrum layering, the negative pressure of utilizing Vacuum Pumps Station to produce is extracted supernatant liquid out.The solution of extracting out is treated the unified purified treatment in back.

The making of Fructus Hippophae water: add Fructus Hippophae extractum to no longer only dissolving in the water of certain volume, filtered through gauze promptly.

Hydrargyrum mixes with the liquid-liquid of stallion urine, Fructus Hippophae water: toward 8.00 liters of blue color stallions urine, 10.00 liters of Fructus Hippophae water that the interior injection of the double glazing reactor that fills hydrargyrum was gathered before 15 days, open electronic stirring, stop after stirring 1 hour under the 540rpm rotating speed.

The liquid-liquid separation of hydrargyrum and stallion urine, Fructus Hippophae water: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The solution of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and stallion urine, Fructus Hippophae water with separate each triplicate.

Hydrargyrum mixes with the liquid-liquid of cattle urine, Fructus Hippophae water: toward 16.00 liters of cattlees urine, 10.00 liters of Fructus Hippophae water that the interior injection of the double glazing reactor that fills hydrargyrum was gathered before 15 days, open electronic stirring, stop after stirring 1 hour under the 540rpm rotating speed.

The liquid-liquid separation of hydrargyrum and cattle urine, Fructus Hippophae water: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The solution of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and cattle urine, Fructus Hippophae water with separate each triplicate.

Hydrargyrum mixes with the liquid-liquid of Alumen preparata, fibroferritum water: inject 7.50 liters of Alumen preparata water and 7.50 liters of fibroferritum water in the double glazing reactor that fills hydrargyrum, open electronic stirring, stop after stirring 1 hour under the 540rpm rotating speed.

The liquid-liquid separation of hydrargyrum and Alumen preparata, fibroferritum water: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The solution of extracting out is treated the unified purified treatment in back.

The making of Alumen preparata water: 1.00 kilograms of Alumen preparata are dissolved in 7.50 premium on currency, and filtered through gauze promptly.

The making of fibroferritum water: 1.00 kilograms of fibroferritum are dissolved in 7.50 premium on currency, and filtered through gauze promptly.

The mixing of hydrargyrum and Alumen preparata, fibroferritum water with separate each triplicate.

Liquid-the liquid of hydrargyrum and Borax, healthy middle-aged male urine mixes: the 50 gram Boraxs of packing in the double glazing reactor that fills hydrargyrum, 5.00 liters of healthy middle-aged males are urinated, and open electronic stirring, stop after 1 hour in stirring under the 540rpm rotating speed.

The liquid-liquid separation of hydrargyrum and Borax, healthy middle-aged male urine: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid solution is extracted out.The liquid of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and Borax, healthy middle-aged male urine with separate each triplicate.

Hydrargyrum mixes with the liquid-liquid of natural salt, tibet red salt, nitre, thenardite, Natrii Sulfas, Sal, trona, Fructus Hippophae water: the 0.30 kilogram of natural salt of packing in the double glazing reactor that fills hydrargyrum, 0.30 kilogram of tibet red salt, 0.30 kilogram of nitre, 0.30 kilogram of thenardite, 0.30 kg of water Natrii Sulfas, 0.50 kilogram of Sal, 0.50 kilogram of trona, 10.00 liters of Fructus Hippophae water and 16.00 intensification water, open electronic stirring, after stirring 1 hour under the 540rpm rotating speed, stop.

The liquid-liquid separation of hydrargyrum and natural salt, tibet red salt, nitre, thenardite, Natrii Sulfas, Sal, trona, Fructus Hippophae water: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The solution of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and natural salt, tibet red salt, nitre, thenardite, Natrii Sulfas, Sal, trona, Fructus Hippophae water with separate each triplicate.

Hydrargyrum mixes with liquid-liquid of cellar, Fructus Hippophae water, Alumen preparata Tu Shui: inject 8.00 liters of cellars, 4.00 liters of Fructus Hippophae water, 16.00 liters of Alumen preparata Tu Shui in the double glazing reactor that fills hydrargyrum, open electronic stirring, stop after stirring 1 hour under the 540rpm rotating speed.

The liquid-liquid separation of hydrargyrum and cellar, Fructus Hippophae water, Alumen preparata Tu Shui: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The solution of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and the solution of cellar, Fructus Hippophae water, Alumen preparata Tu Shui with separate each triplicate.

Hydrargyrum mixes with the liquid-liquid of a watt powder cream, Fructus Hippophae water: pack 1.50 kilograms of watts of powder cream water, 1.00 liters of Fructus Hippophae water and an amount of warm water into to being higher than hydrargyrum face 2～3 centimeters in the double glazing reactor that fills hydrargyrum, open electronic stirring, after stirring 1 hour under the 540rpm rotating speed, stop.

The liquid-liquid separation of hydrargyrum and watt powder cream, Fructus Hippophae water: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The solution of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and a watt powder cream, Fructus Hippophae water with separate each triplicate.

The making of watt powder cream water: 0.10 kilogram of watt of powder of 100 purposes is joined in 1.00 liters of pure water, boil 10 minutes after, with filtered through gauze promptly.

Hydrargyrum mixes with the liquid-liquid of fresh cellar: the 35 ℃ of 10.00 liters of fresh cellars of packing in the double glazing reactor that fills hydrargyrum, open electronic stirring, and after stirring 1 hour under the 540rpm rotating speed, stop.

The liquid-liquid separation of hydrargyrum and fresh cellar: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The solution of extracting out is treated the unified purified treatment in back.

Hydrargyrum respectively repeats twice with separating with the mixing of fresh cellar.

Hydrargyrum mixes with the liquid-liquid of Bulbus Allii water: the 5.00 liters of Bulbus Allii water of packing in the double glazing reactor that fills hydrargyrum, open electronic stirring, and after stirring 1 hour under the 540rpm rotating speed, stop.

The making of Bulbus Allii water: the section of 5.00 kilograms of Bulbus Alliis is joined in 20.00 premium on currency, boil 30 minutes after, with filtered through gauze promptly.

The liquid-liquid separation of hydrargyrum and Bulbus Allii water: after treating supernatant liquid and hydrargyrum layering, supernatant liquid is extracted out with negative pressure.The liquid of extracting out is treated the unified purified treatment in back.

Hydrargyrum respectively repeats four times with the mixing of Bulbus Allii water with separating.

Hydrargyrum mixes with the liquid-liquid of beef water: the 15.00 liters of beef water of packing in the double glazing reactor that fills hydrargyrum, open electronic stirring, and after stirring 1 hour under the 540rpm rotating speed, stop.

The making of beef water: 10.0 kilograms of fat-free beef of size as the Semen Glycines are joined in 30.00 premium on currency, boil 30 minutes after, with filtered through gauze promptly.

The liquid-liquid separation of hydrargyrum and beef water: after treating supernatant liquid and hydrargyrum layering, supernatant liquid is extracted out with negative pressure.The liquid of extracting out is treated the unified purified treatment in back.

Hydrargyrum respectively repeats twice with separating with the mixing of beef water.

Hydrargyrum mixes with the liquid-liquid of butter water: the 5.00 liters of butter water of packing in the double glazing reactor that fills hydrargyrum, open electronic stirring, and after stirring 1 hour under the 540rpm rotating speed, stop.

The making of butter water: 1.00 kilograms of butter are joined in 15.00 premium on currency, boil 20 minutes after, with filtered through gauze promptly.

The liquid-liquid separation of hydrargyrum and butter water: after treating supernatant liquid and hydrargyrum layering, supernatant liquid is extracted out with negative pressure.The liquid of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and butter water with separate each triplicate.

The hydrargyrum of handling through above-mentioned operation is that the moon is photochromic, agglomerating force strong, it is fragmentary to be difficult for, and inserts with splint or chopsticks, can erect.

Hydrargyrum with coagulate mixed liquor, black earth vitriol water, Fructus Hippophae water, the distillation and reflux of cellar in broken Mirabilitum crystallina that leather gets by Adeps Naemorhedi, woodchuck oil, Medulla Bovis seu Bubali, sheep bone marrow, milk: after in the double glazing reactor of band condensing unit, evenly laying the Mirabilitum crystallina of size as the 2.0 cm thick rice, hydrargyrum is slowly imported in the double glazing reactor, subsequently 2.00 liters of mixed liquors, 1.00 liters of Alumen preparata Tu Shui, 1.00 liters of Fructus Hippophae water, 1.00 liters of cellars are slowly imported, open condensing unit, be heated to 80 ℃, react and stop after 72 hours.

The making of mixed liquor: will wait Adeps Naemorhedi, woodchuck oil, Medulla Bovis seu Bubali, sheep bone marrow, the milk of weight to coagulate heat fused such as skin, promptly with filtered through gauze.

Hydrargyrum and the liquid-liquid separation that coagulates mixed liquor that leather gets, black earth vitriol water, Fructus Hippophae water, cellar by Adeps Naemorhedi, woodchuck oil, Medulla Bovis seu Bubali, sheep bone marrow, milk: after treating supernatant liquid and hydrargyrum supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The liquid of extracting out is treated the unified purified treatment in back.

Hydrargyrum and the solution that makes by Bayuan powder and another name of the sun head powder, black earth vitriol water, Fructus Hippophae water, cellar, the distillation and reflux of blue or green oil in Mirabilitum crystallina: after in the double glazing reactor of band condensing unit, evenly laying the Mirabilitum crystallina of size as the 2.0 cm thick rice, slowly import the good hydrargyrum of previous processed, subsequently 2.00 liters of solution, 2.00 liters of Alumen preparata Tu Shui, 2.00 liters of Fructus Hippophae water, 2.00 liters of cellars, 3.00 liters of blue or green oil that made by Bayuan powder and another name of the sun head powder are slowly imported in the lump, open condensing unit, be heated to 150 ℃, react and stop after 12 hours.

The making of the solution that Bayuan powder and another name of the sun head powder make: 0.188 kilogram of Pyritum, 0.188 kilogram of Gold Ore, 0.188 kg silver Ore, 0.188 kilogram of Magnetitum, 0.188 kilogram of Alumen, 0.188 kilogram of sulphur, 0.188 kilogram of Realgar, 0.75 kilogram of Muscovitum, 0.05 kilogram of another name of the sun head powder are joined in 4.00 premium on currency, after the heated and boiled 24 hours, filtered through gauze promptly.

Hydrargyrum and the solution that makes by Bayuan powder and another name of the sun head powder, black earth vitriol water, Fructus Hippophae water, cellar, blue or green oily liquid-liquid separation: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out, then, fall Mirabilitum crystallina with filtered through gauze.The liquid of extracting out is treated the unified purified treatment in back.

Hydrargyrum and eight bronzes, Radix Aconiti Kusnezoffii powder, Oleum Tiglii, the distillation and reflux of black blue or green oil in broken Mirabilitum crystallina: after in the double glazing reactor of band condensing unit, evenly laying the Mirabilitum crystallina of size as the 2.0 cm thick rice, the hydrargyrum that previous processed is good slowly imports the double glazing reactor, add 150 gram Radix Aconiti Kusnezoffii powder, eight bronzes respectively 188 grams, 0.58 liter of Oleum Tiglii, an amount of black blue or green oily again to high 2.0 centimeters of hydrargyrum face, open condensing unit, be heated to 220 ℃ of violent boilings, react and stop after 6 hours.

The making of Radix Aconiti Kusnezoffii powder: with small-sized Chinese medicine grinder with 200 gram Radix Aconiti Kusnezoffii coarse pulverizations after, add 50 milliliters of cellars coarse powder stirred into paste, be ground into 100 order fine powders after drying again.

The liquid-liquid separation of hydrargyrum and eight bronzes, Radix Aconiti Kusnezoffii powder, Oleum Tiglii, black blue or green oil: after treating supernatant liquid and hydrargyrum layering, supernatant liquid is extracted out with negative pressure.The solution of extracting out is treated the unified purified treatment in back.

Hydrargyrum and Cosan liquid-solid is mixed to blue black powder: 35 kilograms of hydrargyrums of handling well and 70 kilogram of 80 purpose Cosan are packed in 150 liters the ball mill of band heater in the lump, after 12 hours, get blue black powder after 3 hours at 80 ℃ of ball millings at room-temperature ball-milling again.

Gu consolidate-mixing of blue black powder and eight bronzes, Bayuan powder, an amount of warm water: with respectively 0.66 kilogram of 100 kilograms of blue black powders, eight bronze, Bayuan powder respectively 0.66 kilogram and suitable quantity of water pack in the lump in the ball mill, ball milling stopped after 12 hours.

The present invention is in order to prevent that mercury vapor overflows the harm operator in the concocting process, and all operations is all finished in hermetic container and container is connected with Vacuum Pumps Station, is in-0.1 atmospheric pressure negative pressure state.Waste water, the waste residue that the aerofluxus of Vacuum Pumps Station and concocting process the produce municipal processing system of to be allowed for access through purified treatment and through after the assay was approved.

In order to guarantee the concocted quality of ZUOTAI, can increase washing step after the liquid-liquid separation operation of the present invention, washing is the process that water or the warm water hydrargyrum after to liquid-liquid separation washs out decontamination.In addition, hydrargyrum spends the night when depositing, and steep with the Fructus Hippophae water logging.

Embodiment two

Hydrargyrum mixes with the liquid-solid of three hot powder: it is that 150 liters, material are in the cone-type mixer of 361L that volume is gone in 5.50 kilograms of Fructus Piperis Longi powder, 4.00 kilograms of Rhizoma Alpiniae Officinarum powder, 5.00 kilograms of Fructus Piperis powders and 50.00 kg of water snow covers, open electronic stirring, when color becomes bottle green, stopped in 24 hours in stirring under the 30rpm rotating speed.

The liquid-liquid separation of hydrargyrum and three Xin Fenshui: inject 30 liters of 70 ℃ of hot water toward cone-type mixer, open electronic stirring, after stirring under the 30rpm rotating speed stops after 10 minutes, treats supernatant liquid and hydrargyrum layering, supernatant liquid is extracted out with the granule pump.The liquid of extracting out is treated the unified purified treatment in back.

Hydrargyrum mixes with the liquid-solid of Sal, trona: 25.00 kilograms of Sal and 25.00 kilograms of trona are packed into to be filled in the cone-type mixer of hydrargyrum, opens electronic stirring, stops after stirring 9 hours under the 30rpm rotating speed.

The liquid-liquid separation of hydrargyrum and Sal, trona water: inject 20.00 liters of 70 ℃ of hot water toward cone-type mixer, open electronic stirring, after stirring 10 minutes under the 30rpm rotating speed, stop, after treating supernatant liquid and hydrargyrum layering, with negative pressure supernatant liquid is extracted out, open bottom valve then, hydrargyrum is sucked in the stainless steel cauldron of subsequent processing.The liquid of extracting out is treated the unified purified treatment in back.

Hydrargyrum mixes with the liquid-liquid of urine of baby boys: 8.00 liters of urine of baby boys gathering before 1 hour are injected fill in 50 liters the stainless steel cauldron of hydrargyrum, open electronic stirring, stop after stirring 9 hours under the 60rpm rotating speed.

The liquid-liquid separation of hydrargyrum and urine of baby boys: after treating supernatant liquid and hydrargyrum layering, the negative pressure of utilizing Vacuum Pumps Station to produce is extracted supernatant liquid out.The liquid of extracting out is treated the unified purified treatment in back.

Hydrargyrum mixes with the liquid-liquid of trona, Fructus Hippophae water: pack in the stainless steel cauldron that fills hydrargyrum 0.10 kilogram of trona and 10.00 liters of Fructus Hippophae water, open electronic stirring, and after stirring 9 hours under the 60rpm rotating speed, stop.

The making of Fructus Hippophae water: add Fructus Hippophae extractum to no longer only dissolving in the water of certain volume, filtered through gauze promptly.

The liquid-liquid separation of hydrargyrum and trona, Fructus Hippophae water: after treating supernatant liquid and hydrargyrum layering, the negative pressure of utilizing Vacuum Pumps Station to produce is extracted supernatant liquid out.The solution of extracting out is treated the unified purified treatment in back.

Hydrargyrum mixes with the liquid-liquid of stallion urine, Fructus Hippophae water: toward 8.00 liters of blue color stallions urine, 10.00 liters of Fructus Hippophae water that the interior injection of the stainless steel cauldron that fills hydrargyrum was gathered before 1 hour, open electronic stirring, stop after stirring 24 hours under the 60rpm rotating speed.

The liquid-liquid separation of hydrargyrum and stallion urine, Fructus Hippophae water: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The solution of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and stallion urine, Fructus Hippophae water with separate each triplicate.

Hydrargyrum mixes with the liquid-liquid of cattle urine, Fructus Hippophae water: toward 16.00 liters of cattlees urine, 10.00 liters of Fructus Hippophae water that the interior injection of the stainless steel cauldron that fills hydrargyrum was gathered before 1 hour, open electronic stirring, stop after stirring 4 hours under the 60rpm rotating speed.

The liquid-liquid separation of the solution of hydrargyrum and cattle urine, Fructus Hippophae water: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The solution of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and cattle urine, Fructus Hippophae water with separate each triplicate.

Hydrargyrum mixes with the liquid-liquid of Alumen preparata, fibroferritum water: inject 7.50 liters of Alumen preparata water and 7.50 liters of fibroferritum water in the stainless steel cauldron that fills hydrargyrum, open electronic stirring, stop after stirring 4 hours under the 60rpm rotating speed.

The making of Alumen preparata water: 1.00 kilograms of Alumen preparata are dissolved in 7.50 premium on currency, and filtered through gauze promptly.

The making of fibroferritum water: 1.00 kilograms of fibroferritum are dissolved in 7.50 premium on currency, and filtered through gauze promptly.

The liquid-liquid separation of hydrargyrum and Alumen preparata, fibroferritum water: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The solution of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and Alumen preparata, fibroferritum water with separate each triplicate.

Liquid-the liquid of hydrargyrum and Borax, healthy middle-aged male urine mixes: the 50 gram Boraxs of packing in the stainless steel cauldron that fills hydrargyrum, 5.00 liters of healthy middle-aged males are urinated, and open electronic stirring, stop after 4 hours in stirring under the 60rpm rotating speed.

The liquid-liquid separation of hydrargyrum and Borax, healthy middle-aged male urine: after supernatant liquid and the hydrargyrum layering, utilize negative pressure that supernatant liquid solution is extracted out.The liquid of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and Borax, healthy middle-aged male urine with separate each triplicate.

Hydrargyrum mixes with the liquid-liquid of natural salt, tibet red salt, nitre, thenardite, Natrii Sulfas, Sal, trona, Fructus Hippophae water: the 0.30 kilogram of natural salt of packing in the stainless steel cauldron that fills hydrargyrum, 0.3 kilogram of tibet red salt, 0.30 kilogram of nitre, 0.30 kilogram of thenardite, 0.30 kg of water Natrii Sulfas, 0.50 kilogram of Sal, 0.50 kilogram of trona, 10.00 liters of Fructus Hippophae water and 16.00 intensification water, open electronic stirring, after stirring 4 hours under the 60rpm rotating speed, stop.

The liquid-liquid separation of hydrargyrum and natural salt, tibet red salt, nitre, thenardite, Natrii Sulfas, Sal, trona, Fructus Hippophae water: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The solution of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and natural salt, tibet red salt, nitre, thenardite, Natrii Sulfas, Sal, trona, Fructus Hippophae water with separate each triplicate.

Hydrargyrum mixes with liquid-liquid of cellar, Fructus Hippophae water, Alumen preparata Tu Shui: inject 8.00 liters of cellars, 4.00 liters of Fructus Hippophae water, 16.00 liters of Alumen preparata Tu Shui in the stainless steel cauldron that fills hydrargyrum, open electronic stirring, stop after stirring 4 hours under the 60rpm rotating speed.

The liquid-liquid separation of hydrargyrum and cellar, Fructus Hippophae water, Alumen preparata Tu Shui: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The solution of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and cellar, Fructus Hippophae water, Alumen preparata Tu Shui with separate each triplicate.

Hydrargyrum mixes with the liquid-liquid of a watt powder cream, Fructus Hippophae water: pack 1.50 kilograms of watts of powder cream water, 1.00 liters of Fructus Hippophae water and an amount of warm water into to being higher than hydrargyrum face 2～3 centimeters in the stainless steel cauldron that fills hydrargyrum, open electronic stirring, after stirring 4 hours under the 60rpm rotating speed, stop.

The making of watt powder cream water: 0.10 kilogram of watt of powder of 100 purposes is joined in 1.00 liters of pure water, be heated to boiling after, with filtered through gauze promptly.

The liquid-liquid separation of hydrargyrum and watt powder cream, Fructus Hippophae water: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The solution of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and a watt powder cream, Fructus Hippophae water with separate each triplicate.

Hydrargyrum mixes with the liquid-liquid of fresh cellar: the 15 ℃ of 10.00 liters of fresh cellars of packing in the stainless steel cauldron that fills hydrargyrum, open electronic stirring, and after stirring 4 hours under the 60rpm rotating speed, stop.

The liquid-liquid separation of hydrargyrum and fresh cellar: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The solution of extracting out is treated the unified purified treatment in back.

Hydrargyrum respectively repeats twice with separating with the mixing of fresh cellar.

Hydrargyrum mixes with the liquid-liquid of Bulbus Allii water: the 5.00 liters of Bulbus Allii water of packing in the stainless steel cauldron that fills hydrargyrum, open electronic stirring, and after stirring 4 hours under the 60rpm rotating speed, stop.

The making of Bulbus Allii water: the section of 5.00 kilograms of Bulbus Alliis is added in 20.00 premium on currency, boil 30 minutes after, with filtered through gauze promptly.

The liquid-liquid separation of hydrargyrum and Bulbus Allii water: after treating supernatant liquid and hydrargyrum layering, supernatant liquid is extracted out with negative pressure.The liquid of extracting out is treated the unified purified treatment in back.

Hydrargyrum respectively repeats four times with the mixing of Bulbus Allii water with separating.

Hydrargyrum mixes with the liquid-liquid of beef water: the 15.00 liters of beef water of packing in the stainless steel cauldron that fills hydrargyrum, open electronic stirring, and after stirring 2 hours under the 60rpm rotating speed, stop.

The making of beef water: 10.0 kilograms of fat-free beef of size as the Semen Glycines are joined in 30.00 premium on currency, boil 30 minutes after, with filtered through gauze promptly.

The liquid-liquid separation of hydrargyrum and beef water: after treating supernatant liquid and hydrargyrum layering, supernatant liquid is extracted out with negative pressure.The liquid of extracting out is treated the unified purified treatment in back.

Hydrargyrum respectively repeats twice with separating with the mixing of beef water.

Hydrargyrum mixes with the liquid-liquid of butter water: the 5.00 liters of butter water of packing in the stainless steel cauldron that fills hydrargyrum, open electronic stirring, and after stirring 2 hours under the 60rpm rotating speed, stop.

The making of butter water: 1.00 kilograms of butter are joined in 15.00 premium on currency, boil 20 minutes after, with filtered through gauze promptly.

The liquid-liquid separation of hydrargyrum and butter water: after treating supernatant liquid and hydrargyrum layering, supernatant liquid is extracted out with negative pressure.The liquid of extracting out is treated the unified purified treatment in back.

The mixing of hydrargyrum and butter water with separate each triplicate.

The hydrargyrum of handling through above-mentioned operation is that the moon is photochromic, agglomerating force strong, it is fragmentary to be difficult for, and inserts with splint or chopsticks, can erect.

Hydrargyrum with coagulate mixed liquor, black earth vitriol water, Fructus Hippophae water, the distillation and reflux of cellar in broken Mirabilitum crystallina that leather gets by Adeps Naemorhedi, woodchuck oil, Medulla Bovis seu Bubali, sheep bone marrow, milk: after in the stainless steel cauldron of band condensing unit, evenly laying the Mirabilitum crystallina of size as the 2.0 cm thick rice, slowly import hydrargyrum in the stainless steel cauldron, subsequently 2.00 liters of mixed liquors, 1.00 liters of Alumen preparata Tu Shui, 1.00 liters of Fructus Hippophae water, 1.00 liters of cellars are slowly imported, open condensing unit, be heated to 150 ℃, react and stop after 12 hours.

The making of mixed liquor: will wait Adeps Naemorhedi, woodchuck oil, Medulla Bovis seu Bubali, sheep bone marrow, the milk of weight to coagulate the skin heat fused, promptly with filtered through gauze.

Hydrargyrum and the liquid-liquid separation that coagulates mixed liquor that leather gets, black earth vitriol water, Fructus Hippophae water, cellar by Adeps Naemorhedi, woodchuck oil, Medulla Bovis seu Bubali, sheep bone marrow, milk: after treating supernatant liquid and hydrargyrum supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out.The liquid of extracting out is treated the unified purified treatment in back.

Hydrargyrum and the solution that makes by Bayuan powder and another name of the sun head powder, black earth vitriol water, Fructus Hippophae water, cellar, the distillation and reflux of blue or green oil in Mirabilitum crystallina: after in the stainless steel cauldron of band condensing unit, evenly laying the Mirabilitum crystallina of size as the 2.0 cm thick rice, slowly import the good hydrargyrum of previous processed, subsequently 2.00 liters of solution, 2.00 liters of Alumen preparata Tu Shui, 2.00 liters of Fructus Hippophae water, 2.00 liters of cellars, 3.00 liters of blue or green oil that made by Bayuan powder and another name of the sun head powder are slowly imported in the lump, open condensing unit, be heated to 80 ℃, react and stop after 72 hours.

The making of the solution that Bayuan powder and another name of the sun head powder make: 0.188 kilogram of Pyritum, 0.188 kilogram of Gold Ore, 0.188 kg silver Ore, 0.188 kilogram of Magnetitum, 0.188 kilogram of Alumen, 0.188 kilogram of sulphur, 0.188 kilogram of Realgar, 0.75 kilogram of Muscovitum, 0.05 kilogram of another name of the sun head powder are joined in 4.00 premium on currency, after the heated and boiled 24 hours, filtered through gauze promptly.

Hydrargyrum and the solution that makes by Bayuan powder and another name of the sun head powder, black earth vitriol water, Fructus Hippophae water, cellar, blue or green oily liquid-liquid separation: after treating supernatant liquid and hydrargyrum layering, utilize negative pressure that supernatant liquid is extracted out, then, fall Mirabilitum crystallina with filtered through gauze.The liquid of extracting out is treated the unified purified treatment in back.

Hydrargyrum and eight bronzes, Radix Aconiti Kusnezoffii powder, Oleum Tiglii, the distillation and reflux of black blue or green oil in broken Mirabilitum crystallina: after in the stainless steel cauldron of band condensing unit, evenly laying the Mirabilitum crystallina of size as the 2.0 cm thick rice, the hydrargyrum that previous processed is good slowly imports stainless steel cauldron, add 150 gram Radix Aconiti Kusnezoffii powder, eight bronzes respectively 188 grams, 0.58 liter of Oleum Tiglii, an amount of black blue or green oily again to high 2.0 centimeters of hydrargyrum face, open condensing unit, be heated to 120 ℃ of violent boilings, react and stop after 24 hours.

The making of Radix Aconiti Kusnezoffii powder: with small-sized Chinese medicine grinder with 200 gram Radix Aconiti Kusnezoffii coarse pulverizations after, add 50 milliliters of cellars coarse powder stirred into paste, be ground into 100 order fine powders after drying again.

The liquid-liquid separation of hydrargyrum and eight bronzes, Radix Aconiti Kusnezoffii powder, Oleum Tiglii, black blue or green oil: after treating supernatant liquid and hydrargyrum layering, supernatant liquid is extracted out with negative pressure.The solution of extracting out is treated the unified purified treatment in back.

Hydrargyrum and Cosan liquid-solid is mixed to blue black powder: 35 kilograms of hydrargyrums of handling well and 70 kilogram of 80 purpose Cosan are packed in 150 liters the cone-type mixer of band heater in the lump, after 48 hours, get blue black powder after 6 hours at 80 ℃ of ball millings at room-temperature ball-milling more earlier.

Gu consolidate-mixing of blue black powder and eight bronzes, Bayuan powder, an amount of warm water: with respectively 0.66 kilogram of 100 kilograms of blue black powders, eight bronze, Bayuan powder respectively 0.66 kilogram and suitable quantity of water pack in the lump in the cone-type mixer, ball milling stopped after 48 hours.

The present invention is in order to prevent that mercury vapor overflows the harm operator in the concocting process, and all operations is all finished in hermetic container and container is connected with Vacuum Pumps Station, is in-0.5 atmospheric negative pressure state.Waste water, the waste residue that the aerofluxus of Vacuum Pumps Station and concocting process the produce municipal processing system of to be allowed for access through purified treatment and through after the assay was approved.

In order to guarantee the concocted quality of ZUOTAI, can increase washing step after the liquid-liquid separation operation of the present invention, washing is the process that water or the warm water hydrargyrum after to liquid-liquid separation washs out decontamination.In addition, hydrargyrum spends the night when depositing, and steep with the Fructus Hippophae water logging.