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CN109135145A - It is a kind of using mixing polysaccharide glue as thin slice spontaneous heating body of thickener and preparation method thereof - Google Patents

️Fri Jan 04 2019

It is a kind of using mixing polysaccharide glue as thin slice spontaneous heating body of thickener and preparation method thereof Download PDF

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Publication number

CN109135145A

CN109135145A CN201810946691.2A CN201810946691A CN109135145A CN 109135145 A CN109135145 A CN 109135145A CN 201810946691 A CN201810946691 A CN 201810946691A CN 109135145 A CN109135145 A CN 109135145A Authority

China

Prior art keywords

thickener

polysaccharide glue

mixing polysaccharide

thin slice

heating body

Prior art date

2018-08-20

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Pending

Application number

CN201810946691.2A

Other languages

Chinese (zh)

Inventor

汤小雄

孙经

孙经一

徐发展

刘宝宝

张冬

陈鹏

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

SHANGHAI WARMYOU INDUSTRIAL Co Ltd

Original Assignee

SHANGHAI WARMYOU INDUSTRIAL Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2018-08-20

Filing date

2018-08-20

Publication date

2019-01-04

2018-08-20 Application filed by SHANGHAI WARMYOU INDUSTRIAL Co Ltd filed Critical SHANGHAI WARMYOU INDUSTRIAL Co Ltd

2018-08-20 Priority to CN201810946691.2A priority Critical patent/CN109135145A/en

2019-01-04 Publication of CN109135145A publication Critical patent/CN109135145A/en

Status Pending legal-status Critical Current

Links

239000003292 glue Substances 0.000 title claims abstract description 42
238000002156 mixing Methods 0.000 title claims abstract description 38
150000004676 glycans Chemical class 0.000 title claims abstract description 37
229920001282 polysaccharide Polymers 0.000 title claims abstract description 37
239000005017 polysaccharide Substances 0.000 title claims abstract description 37
238000010438 heat treatment Methods 0.000 title claims abstract description 20
230000002269 spontaneous effect Effects 0.000 title claims abstract description 19
239000002562 thickening agent Substances 0.000 title claims abstract description 17
238000002360 preparation method Methods 0.000 title claims abstract description 13
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 23
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 19
229920000642 polymer Polymers 0.000 claims abstract description 10
239000002250 absorbent Substances 0.000 claims abstract description 9
230000002745 absorbent Effects 0.000 claims abstract description 9
239000000843 powder Substances 0.000 claims abstract description 9
206010037660 Pyrexia Diseases 0.000 claims abstract description 7
229910052751 metal Inorganic materials 0.000 claims abstract description 7
239000002184 metal Substances 0.000 claims abstract description 7
229920001285 xanthan gum Polymers 0.000 claims description 23
239000000230 xanthan gum Substances 0.000 claims description 23
235000010493 xanthan gum Nutrition 0.000 claims description 23
229940082509 xanthan gum Drugs 0.000 claims description 23
229920002752 Konjac Polymers 0.000 claims description 22
LUEWUZLMQUOBSB-FSKGGBMCSA-N (2s,3s,4s,5s,6r)-2-[(2r,3s,4r,5r,6s)-6-[(2r,3s,4r,5s,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5s,6r)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-4,5-dihydroxy-2-(hydroxymethyl)oxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@@H](O[C@@H]2[C@H](O[C@@H](OC3[C@H](O[C@@H](O)[C@@H](O)[C@H]3O)CO)[C@@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-FSKGGBMCSA-N 0.000 claims description 17
241001312219 Amorphophallus konjac Species 0.000 claims description 17
235000001206 Amorphophallus rivieri Nutrition 0.000 claims description 17
229920002581 Glucomannan Polymers 0.000 claims description 17
229940046240 glucomannan Drugs 0.000 claims description 17
239000000252 konjac Substances 0.000 claims description 17
235000010485 konjac Nutrition 0.000 claims description 17
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical group [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 11
229910052799 carbon Inorganic materials 0.000 claims description 11
239000013078 crystal Substances 0.000 claims description 6
WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 4
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 4
238000001035 drying Methods 0.000 claims description 4
229920000058 polyacrylate Polymers 0.000 claims description 4
239000000203 mixture Substances 0.000 claims description 3
UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 2
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 2
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 2
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 2
239000001110 calcium chloride Substances 0.000 claims description 2
229910001628 calcium chloride Inorganic materials 0.000 claims description 2
230000003647 oxidation Effects 0.000 claims description 2
238000007254 oxidation reaction Methods 0.000 claims description 2
239000001103 potassium chloride Substances 0.000 claims description 2
235000011164 potassium chloride Nutrition 0.000 claims description 2
239000010936 titanium Substances 0.000 claims description 2
229910052719 titanium Inorganic materials 0.000 claims description 2
239000000463 material Substances 0.000 abstract description 4
238000004519 manufacturing process Methods 0.000 abstract description 2
239000000243 solution Substances 0.000 description 15
238000003756 stirring Methods 0.000 description 5
239000003643 water by type Substances 0.000 description 5
239000012153 distilled water Substances 0.000 description 4
230000037237 body shape Effects 0.000 description 3
239000003795 chemical substances by application Substances 0.000 description 2
238000004090 dissolution Methods 0.000 description 2
238000005259 measurement Methods 0.000 description 2
238000000034 method Methods 0.000 description 2
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
235000010489 acacia gum Nutrition 0.000 description 1
239000001785 acacia senegal l. willd gum Substances 0.000 description 1
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
230000009286 beneficial effect Effects 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
238000001514 detection method Methods 0.000 description 1
238000010586 diagram Methods 0.000 description 1
238000004821 distillation Methods 0.000 description 1
239000007789 gas Substances 0.000 description 1
239000011259 mixed solution Substances 0.000 description 1
229910052760 oxygen Inorganic materials 0.000 description 1
239000001301 oxygen Substances 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
239000011734 sodium Substances 0.000 description 1
229910052708 sodium Inorganic materials 0.000 description 1
230000002195 synergetic effect Effects 0.000 description 1
238000003786 synthesis reaction Methods 0.000 description 1
230000008719 thickening Effects 0.000 description 1
239000010455 vermiculite Substances 0.000 description 1
229910052902 vermiculite Inorganic materials 0.000 description 1
235000019354 vermiculite Nutrition 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L33/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- C08L33/02—Homopolymers or copolymers of acids; Metal or ammonium salts thereof
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F7/00—Heating or cooling appliances for medical or therapeutic treatment of the human body
- A61F7/02—Compresses or poultices for effecting heating or cooling
- A61F7/03—Compresses or poultices for effecting heating or cooling thermophore, i.e. self-heating, e.g. using a chemical reaction
- A61F7/032—Compresses or poultices for effecting heating or cooling thermophore, i.e. self-heating, e.g. using a chemical reaction using oxygen from the air, e.g. pocket-stoves
- A61F7/034—Flameless
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K5/00—Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
- C09K5/16—Materials undergoing chemical reactions when used
- C09K5/18—Non-reversible chemical reactions
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F7/00—Heating or cooling appliances for medical or therapeutic treatment of the human body
- A61F7/02—Compresses or poultices for effecting heating or cooling
- A61F2007/0203—Cataplasms, poultices or compresses, characterised by their contents; Bags therefor
- A61F2007/0204—Cataplasms, poultices or compresses, characterised by their contents; Bags therefor containing clay, mud, fango, sand, kaolin clay, volcanic or other inorganic granular solids
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F7/00—Heating or cooling appliances for medical or therapeutic treatment of the human body
- A61F7/02—Compresses or poultices for effecting heating or cooling
- A61F2007/0203—Cataplasms, poultices or compresses, characterised by their contents; Bags therefor
- A61F2007/0206—Cataplasms, poultices or compresses, characterised by their contents; Bags therefor containing organic solids or fibres
- A61F2007/0209—Synthetics, e.g. plastics
- A61F2007/0214—Polymers, e.g. water absorbing
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend

Landscapes

Chemical & Material Sciences (AREA)
Health & Medical Sciences (AREA)
Engineering & Computer Science (AREA)
Organic Chemistry (AREA)
Physics & Mathematics (AREA)
Thermal Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
General Health & Medical Sciences (AREA)
Biomedical Technology (AREA)
Animal Behavior & Ethology (AREA)
Vascular Medicine (AREA)
Public Health (AREA)
Veterinary Medicine (AREA)
Heart & Thoracic Surgery (AREA)
Life Sciences & Earth Sciences (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Emergency Medicine (AREA)
General Chemical & Material Sciences (AREA)
Combustion & Propulsion (AREA)
Materials Engineering (AREA)
Cosmetics (AREA)
Medicinal Preparation (AREA)

Abstract

The present invention relates to a kind of using mixing polysaccharide glue as thin slice spontaneous heating body of thickener and preparation method thereof, including following components in weight percent: metal powder 20~60%, activated carbon 1~15%, fever promotor 0.5~8%, water 20~35%, mixing polysaccharide glue 1~10%, water absorbent polymer 10~25%, the sum of percentage of each component are 100%；The sheet type heater thickness that the present invention is formed is uniform, not will cause pocket, powder leakage the problems such as, and reduce the usage amount of thickener, reduce materials cost, be convenient for industrial mass production.

Description

It is a kind of using mixing polysaccharide glue as thin slice spontaneous heating body of thickener and preparation method thereof

Technical field

It is thickening that the present invention relates to a kind of thin slice spontaneous heating bodies and preparation method thereof, more particularly to one kind with mixing polysaccharide glue Thin slice spontaneous heating body of agent and preparation method thereof.

Background technique

Spontaneous heating body is warm paste (paddy claims " warmer ", " heating packet ", " a patch heat " etc.), is the pass for human body warm The basic principle of key material, fever is: by the polymer containing synthesis such as iron powder, active carbon, inorganic salts, vermiculite, water, in sky Exothermic chemical reaction independently occurs in gas under the action of oxygen, it is sustainable 12~20 hours general.

Mainly there is the two major classes type of sheet type and powdery in existing product, is thickened used in existing sheet type heater Agent is xanthan gum or Arabic gum etc., and still, under comparable sodium, the viscosity of monistic glue is not strong, and when use needs to be added big The unicity glue of amount makes the materials increased costs of glue.

Summary of the invention

To solve problems of the prior art, the invention of this hair provides a kind of using mixing polysaccharide glue as the thin of thickener Piece spontaneous heating body and preparation method thereof is to solve the above problems.

Present invention firstly relates to a kind of mixing polysaccharide glue；

The mixing polysaccharide glue, is mixed with konjac glucomannan by xanthan gum and is constituted.

The xanthan gum uses the preparation method that colloidal sol is blended with the konjac glucomannan, specifically, including the following steps:

(1) it by xanthan gum and konjac glucomannan, is separately added into equal amount of distilled water and dissolves；

(2) konjaku sol solution is mixed again with xanthan gum solution, is put into 70~90 DEG C of waters bath with thermostatic control, with homogenizer constant temperature It is stirred 25~35min, stops stirring, after keeping the temperature 25~35min, is cooled to room temperature and can be obtained mixing polysaccharide glue.

The weight ratio of the dosage of each component are as follows:

Xanthan gum: konjac glucomannan=7:2~4, preferably 7:3；

Total dosage of water is 100~125 times, preferably 100 times of the sum of xanthan gum and konjac glucomannan weight；

Described is a kind of using mixing polysaccharide glue as the thin slice spontaneous heating body of thickener, with a thickness of 1mm~4mm, including it is as follows Components in weight percent:

The sum of percentage of each component is 100%；

Preferably, the metal powder is iron powder, but is not limited only to iron powder, can also utilize magnesium powder, titanium valve, zinc powder etc. Other oxidation heat liberation metal powders；

Preferably, the active carbon is adopted as carbon crystal, but is not limited only to carbon crystal, can also be using other carbon structures Body；

Preferably, the fever promotor also can be used potassium chloride, calcium chloride etc., both may be used using Nacl To be used alone, but also also mix together；

Preferably, the water absorbent polymer is using polyacrylate series；

It is a kind of using mixing polysaccharide glue as the preparation method of the thin slice spontaneous heating body of thickener:

(1) the mixing polysaccharide glue, activated carbon and water absorbent polymer are mixed under room temperature, obtain paste.

(2) iron powder and fever promotor are added under room temperature to be stirred, is compressed into tablet form or needs other vertical Body shape, then under 700~720 support vacuum degrees, 80~100 DEG C drying 5~7 hours, can be obtained product.

Beneficial effects of the present invention:

The sheet type heater thickness that the present invention is formed is uniform, not will cause pocket, powder leakage the problems such as, and reduce increasing Thick dose of usage amount reduces materials cost, is convenient for industrial mass production.

Detailed description of the invention

Fig. 1 is concentration-viscosity change curve comparison diagram of mixing polysaccharide glue and unicity glue.

Specific embodiment

Embodiment 1

The preparation of mixing polysaccharide glue:

(1) it by xanthan gum and konjac glucomannan, is separately added into equal amount of distilled water and dissolves；

(2) konjaku sol solution is mixed again with xanthan gum solution, is put into 80 DEG C of waters bath with thermostatic control, stirred with homogenizer constant temperature 30min is mixed, stirring is stopped, after keeping the temperature 30min, is cooled to room temperature and can be obtained mixing polysaccharide glue.

The weight ratio of the dosage of each component are as follows:

Xanthan gum: konjac glucomannan=7:3；

Total dosage of water is 100 times of the sum of xanthan gum and konjac glucomannan weight；

The personal style and attitude that homogenizer uses Guangzhou Lai Kang Science and Technology Ltd. to provide removes homogenizer for TUL.

It is a kind of using mixing polysaccharide glue as the thin slice spontaneous heating body of thickener, compare group with a thickness of 2mm, including following weight hundred Part:

Metal powder is iron powder, and active carbon is adopted as carbon crystal, and the promotor that generates heat using Nacl, adopt by water absorbent polymer With polyacrylate series.

Preparation method:

(1) the mixing polysaccharide glue, activated carbon and water absorbent polymer are mixed under room temperature, obtain paste.

(2) iron powder and fever promotor are added under room temperature to be stirred, is compressed into tablet form or needs other vertical Body shape, then under 720 support vacuum degrees, 90 DEG C drying 6 hours, can be obtained product.

Embodiment two

The preparation of mixing polysaccharide glue:

(1) it by xanthan gum and konjac glucomannan, is separately added into equal amount of distilled water and dissolves；

(2) konjaku sol solution is mixed again with xanthan gum solution, is put into 70 DEG C of waters bath with thermostatic control, stirred with homogenizer constant temperature 30min is mixed, stirring is stopped, after keeping the temperature 30min, is cooled to room temperature and can be obtained mixing polysaccharide glue.

The weight ratio of the dosage of each component are as follows:

Xanthan gum: konjac glucomannan=7:2；

Total dosage of water is 120 times of the sum of xanthan gum and konjac glucomannan weight；

The personal style and attitude that homogenizer uses Guangzhou Lai Kang Science and Technology Ltd. to provide removes homogenizer for TUL.

It is a kind of using mixing polysaccharide glue as the thin slice spontaneous heating body of thickener, compare group with a thickness of 3mm, including following weight hundred Part:

Metal powder is iron powder, and active carbon is adopted as carbon crystal, and the promotor that generates heat using Nacl, adopt by water absorbent polymer With polyacrylate series.

Preparation method:

(1) the mixing polysaccharide glue, activated carbon and water absorbent polymer are mixed under room temperature, obtain paste.

(2) iron powder and fever promotor are added under room temperature to be stirred, is compressed into tablet form or needs other vertical Body shape, then under 700 support vacuum degrees, 80 DEG C drying 7 hours, can be obtained product.

Embodiment three

The viscosity performance detection method of mixing polysaccharide glue and as a result, as follows:

Under the conditions of identical temperature, the unicity glue and mixing polysaccharide sol solution of various concentration are accurately prepared respectively；

Test equipment: the brand of BROOKFIELD company of the U.S. is used to strangle winged Brookfield LVDV-1M digital display to be rich Viscosimeter measurement.

(1) the mixing polysaccharide sol solution of various concentration is prepared:

Take quantitative xanthan gum and konjac glucomannan respectively, the ratio of xanthan gum and konjac glucomannan is 7:3, is separately added into equivalent distillation Mixed dissolution in water；Konjaku sol solution is mixed with xanthan gum solution again, is put into 80 DEG C of waters bath with thermostatic control, is stirred with homogenizer constant temperature Mix mixing 30min, stop stirring, keep the temperature 30min after, be cooled to room temperature, successively make concentration be 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7%, 0.8%, 0.9%, 1% 10 groups of mixing polysaccharide sol solutions.

(2) the unicity sol solution of various concentration is prepared:

Quantitative xanthan gum is taken, mixed dissolution in quantitative distilled water is added；It is put into 80 DEG C of waters bath with thermostatic control, uses homogenizer Constant temperature is stirred 30min, stops stirring, after keeping the temperature 30min, is cooled to room temperature, successively make concentration be 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7%, 0.8%, 0.9%, 1% 10 groups of xanthan gum solutions.

In above-mentioned identical method, take quantitative konjac glucomannan, successively make concentration be 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7%, 0.8%, 0.9%, 1% 10 groups of konjaku sol solutions.

Measure the unicity glue and mixing polysaccharide of various concentration respectively using Brookfield LVDV-1M digital display viscosimeter The viscosity of sol solution, measurement result is as shown in Figure 1:

As can be seen that the mixed solution of xanthan gum and konjac glucomannan has apparent association from concentration-viscosity change curve Same synergistic effect, the viscosity of mixing polysaccharide glue and the viscosity number of the single glue of same concentration increase again, this performance, that is, increased glue Viscosity, and reduce the usage amount of glue.

Claims (8)

1. a kind of using mixing polysaccharide glue as the thin slice spontaneous heating body of thickener, which is characterized in that with a thickness of 1mm~4mm, including such as Lower components in weight percent:

The sum of percentage of each component is 100%.

2. according to claim 1 using mixing polysaccharide glue as the thin slice spontaneous heating body of thickener, which is characterized in that described Metal powder is iron powder, but is not limited only to iron powder, can also utilize other oxidation heat liberation metal powders such as magnesium powder, titanium valve, zinc powder.

3. according to claim 1 using mixing polysaccharide glue as the thin slice spontaneous heating body of thickener, which is characterized in that described Active carbon is adopted as carbon crystal, but is not limited only to carbon crystal, can also be using other carbon structures.

4. according to claim 1 using mixing polysaccharide glue as the thin slice spontaneous heating body of thickener, which is characterized in that described Promotor generate heat using Nacl, potassium chloride, calcium chloride etc. also can be used, both can be used alone, can also mix It uses.

5. according to claim 1 using mixing polysaccharide glue as the thin slice spontaneous heating body of thickener, which is characterized in that described Mixing polysaccharide glue, which is mixed by xanthan gum with konjac glucomannan, to be constituted.

6. according to claim 5 using mixing polysaccharide glue as the thin slice spontaneous heating body of thickener, which is characterized in that described Xanthan gum and the konjac glucomannan mixed proportion are 7:3.

7. according to claim 1 using mixing polysaccharide glue as the thin slice spontaneous heating body of thickener, which is characterized in that described Water absorbent polymer is using polyacrylate series.

8. a kind of using mixing polysaccharide glue as the thin slice spontaneous heating body preparation method of thickener, which comprises the steps of:

(1) the mixing polysaccharide glue, activated carbon and water absorbent polymer are mixed under room temperature, obtain paste.

(2) iron powder and fever promotor are added under room temperature to be stirred, the other stereo structures for being compressed into tablet form or needing, Again under 700~720 support vacuum degrees, 80~100 DEG C drying 5~7 hours, can be obtained product.

CN201810946691.2A 2018-08-20 2018-08-20 It is a kind of using mixing polysaccharide glue as thin slice spontaneous heating body of thickener and preparation method thereof Pending CN109135145A (en)

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CN201810946691.2A CN109135145A (en)	2018-08-20	2018-08-20	It is a kind of using mixing polysaccharide glue as thin slice spontaneous heating body of thickener and preparation method thereof

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