Pharmacokinetic properties of zolpidem in elderly and young adults: possible modulation by testosterone in men - PubMed
Clinical Trial
Pharmacokinetic properties of zolpidem in elderly and young adults: possible modulation by testosterone in men
Joel O Olubodun et al. Br J Clin Pharmacol. 2003 Sep.
Abstract
Aims: The influence of ageing on the pharmacokinetics of zolpidem, an extensively prescribed hypnotic medication, was evaluated in healthy human volunteers.
Methods: A series of 16 elderly (age: 61-85 years) and 24 young (age: 22-42 years) volunteers received single 5 mg oral doses of zolpidem tartrate. Serum zolpidem concentrations were determined by HPLC with fluorescence detection in samples drawn during 8 h after dosage. The effect of testosterone on zolpidem biotransformation was evaluated in vitro using human liver microsomes. Possible induction of CYP3A protein expression and function was studied in cultured human hepatocytes.
Results: Among men, apparent oral clearance of zolpidem was decreased in elderly compared to young subjects (3.8 vs 11.0 ml min-1 kg-1, P < 0.01), Cmax was increased (93 vs 40 ng ml-1, P < 0.01), and half-life increased (2.7 vs 1.5 h, P < 0.03). Among women, zolpidem oral clearance was decreased in the elderly (3.0 vs 5.8 ml min-1 kg-1, P < 0.02), Cmax increased (108 vs 60 ng ml-1, P < 0.001), with no difference in t1/2 (2.3 vs 2.4 h). Among male subjects, free serum testosterone concentrations were lower in the elderly (10.5 vs 19.0 pg ml-1, P < 0.01), and were significantly correlated with zolpidem clearance (r2 = 0.46, P < 0.001). Multiple regression analysis indicated a greater relative contribution of serum testosterone than age to the oral clearance of zolpidem among men. In human liver microsomes, co-incubation of zolpidem (10 micro m) with varying concentrations of testosterone produced activation of biotransformation of zolpidem to its principal hydroxylated metabolite. Maximum activation was achieved at equimolar concentrations of testosterone (10 micro m). However, testosterone did not induce immunoactive CYP3A4 expression or catalytic function in cultured human hepatocytes.
Conclusions: The increased Cmax and lower oral clearance of zolpidem in the elderly are consistent with recommendations of lower clinical doses of zolpidem in the elderly. Our clinical and in vitro data both suggest that reduced free serum testosterone may have a modulatory role in age-dependent changes in zolpidem pharmacokinetics in men.
Figures

Mean (± SEM) serum zolpidem concentrations–time plots for young (•, ♦) and elderly (○, ◊) male (a) and female (b) volunteers.

Relationship between free serum testosterone concentration and zolpidem oral clearance (top) and zolpidem AUC (bottom) in male subjects. For zolpidem AUC, linear regression was used after logarithmic transformation of AUC values (r2 = 0.43). For zolpidem clearance, the line represents a function of the form: γ = BxA (r2 = 0.46). Elderly male (○) and young male (•).

Effect of testosterone on the rate of formation of the zolpidem M-3 metabolite from zolpidem (10 µ
m, equivalent to 2.88 µg ml−1) by human liver microsomes. Rates of formation are expressed as a percent of the control velocity with no testosterone present. Each point is the mean (± SEM) of four separate human liver microsomal preparations.

Effect of 48 h of exposure to rifampin (20 µ
m) () or testosterone (10 µ
) () on triazolam α-hydroxylation activity and on the expression of immunoactive CYP3A4 protein in human hepatocytes in cell culture. Bars indicate the mean (± SEM) values relative to cells cultured with vehicle control (0.5% DMSO). Asterisk (*) indicates a significant difference from 1.0 based on Student's t-test (n = 4 separate experiments for triazolam α-hydroxylation, n = 2 for immunoactive protein).
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